AN ANALYTICAL XRAY SERVICES LABORATORY
Feel free to call us: 940-784-3002

FCT 0027 Xray decal visual croppedWe’ve been working with XRD machines for about 40 years now and to be quite honest, very little has changed. Most of the really exciting advancements have been software based, but there have certainly been changes to the hardware as well. We’ve introduced a few ourselves such as the KSA-SDD-150 detector. Automatic anti-scatter and divergence slits, additional axes and degrees of control have all increase the versatility of these instruments and opened them up to more advanced and unique experiments, but nothing has had an effect matching the new crop of Position Sensitive Detector (PSD). These have been around for decades, but didn’t really become popular until the a solid state version was introduced. There are still some trade-offs as mentioned in our KSA-SDD-150 post, but when you need speed, a PSD is the way to go.

Until recently, the only option for clients looking for this kind of speed was either a new XRD or a refurbished Bruker D8 system with a LynxEye or Vantec-1. While the D8 is a great machine and the LynxEye is a world class detector, the cost is usually too much for academic or small labs to bear. This has all been changing recently with the introduction of a truly aftermarket detector system from FCT ACTech. No other company that we’re aware of has worked so hard to make their hardware as turnkey as possible so the user isn’t left holding a box of parts and an instruction manual.

We can now offer detector upgrades for D5000 Theta/Theta and D5000 T2T systems with kits soon to be available for D500 systems as well. Software integration with DiffracPlus (standard software for Bruker XRD systems) is seamless and full integration with MDI Datascan is very close to completion. The future is very bright for users of these XRD systems.

Contact us for more information on these detectors


NovaculitesiliconKey features:

  • Data collection at 30x the speed of a standard point detector.
  • Dramatic increase in throughput
  • Plug-and-play retrofit
  • Maintenance free (no gas charge required)
  • Stand-alone operation for custom experiments
  • Excellent angular resolution

 

Technical Specifications:

  • Maximum count rate: 500Kcps / pixcel, 50Mcps global
  • Maximum scanning speed: 120 deg/min
  • Angular resolution: 0.06 deg at 200mm radius
  • Strip pitch: 120um
  • Number of channels: 96
  • Angular span: 3.3 degrees
  • Energy resolution: <10%
  • Energy range: 4.5KeV to 17KeV, efficiency at 30KeV is 10%
  • Compatible with all common XRD tube anodes including Cr, Fe, Co, Cu, Mo and W.

XRD sample holders are easily the most common items we’re asked to machine. Sometimes it’s because they’re no longer available, but usually, it’s to accommodate some special application. Sometimes it’s as simple as making them from Aluminum to allow for cleaning with acetone or other harsh solvents. Other times it has more to do with the clients preferred style of loading or sample volume. The end result is that there’s very little consistency so our process needs to be as versatile as possible. This video highlights the most recent process. It’s hard to see exactly what’s going on through the coolant, but this is a test run of a program to cut special holders for 25mm filter membrane holders for respirable silica measurements (or anything else one might want to deposit onto a 25mm filter). It’s cutting the bottom of one holder and the top of another (each on its own side of the fixture).  A full load of these produces 6 complete holders for every run.

Siemens goniometers are about as sturdy as they come. Large diameter gears and bearings spread out forces across a wide area resulting in smooth and stable performance as well as very high load handling due to the added leverage of this arrangement. For this reason, they’ll run for many years even after the grease inside has become hard and contaminated with dust. Most users don’t even know their goniometer is getting stiff until we check it during a PM. Catching this before the goniometer starts to hang up saves thousands of dollars and weeks of down time. Our goniometer rebuild service involves complete disassembly of the goniometer down to individual ball bearings for a thorough cleaning. We’ve tried to duplicate this procedure on-site with very limited success as the large components are best cleaned in a full size solvent bath and it’s special brackets are required to avoid concentricity issues during reassembly. All the critical electronics are replaced during reassembly along with fresh lubrication. The best case scenario is that we catch issue far enough in advance to get a matching replacement goniometer rebuilt and shipped out. There are too many variants to keep rebuilt units in stock all the time. This way we only need to come to the site once to swap the goniometer and perform the necessary zero alignment. The old goniometer goes back in the same crate and we’re done in a day or two. Waiting till a hard failure of the goniometer means a trip out to identify the problem and disassemble the system. The goniometer is shipped in for a rebuild which can easily take a few days to complete before being shipped back along with a second on-site visit. I’d estimate the extra cost to be right around $6k plus the cost of shipping and two weeks of downtime. We certainly don’t mind going this route, but if it were my money, I’d rather spend it on a comprehensive check of the machine rather than emergency services.

These pictures are from one of our first full rebuilds. This instrument was installed in a D5000-MATIC instrument at a cement plant. I’ve never seen so much dust inside a goniometer. Another particularly rough one was from a horizontal goniometer on a single-crystal system at a university. The students had a terrible habit of breaking Si(100) wafers and dropping them onto the goniometer face. Those little shards made their way into the bearings resulting in a rather perilous rebuild with shards of Si throughout it.